Thursday, January 5, 2017

Manufacture of Ammonia by Haber's process | HSEB Chemistry notes

More on original site : Manufacture of Ammonia by Haber's process

Principle :  In this process , Ammonia is prepared from nitrogen and hydrogen. In ordinary condition , nitrogen do not react with hydrogen but when it is mixed with hydrogen in the ration 1:3 under 450 C temperature and 200-500 atm pressure in presence of Iron as catalyst and Molybdenum as promoter then it combines to form
Ammonia (NH3).




The reaction is exothermic, reversible and proceeding with decrease in volume. So, following condition is needed for better yield of it :

a. Low temperature : The reaction is exothermic , it as a rule is followed by low temperature. But if the temperature is very low then the rate of reaction will
be very slow and production of Ammonia will not be economically fruitful and beneficial. So optimum temperature of 450 C is maintained in this process.

b. high pressure : The reaction is reversible so it favored by high pressure. So pressure of about 200-500 atm is maintained.

c. High concentration : If the reactant are excess the the product formed will also be same . So either hydrogen or nitrogen in the reactant side is made excess to 
produce high amount of ammonia.

d. Use of catalyst : In absence of catalyst, the reaction will be slow. So, Iron is used as catalyst along with molybdenum as promoter to increase the rate of reaction
without hampering it. 


Process : In this process, N2 is treated with H2 in the ratio 1:3 . Then the gaseous mixture is passed through compressor in which pressure of 200-500 atm is applied.
Then the gases mixture is passed through catalyst chamber packed with finely divided Iron + molybdenum. The chamber is initially heated to about 450 C to initiate the 
reaction. During this condition , 15% of the gaseous mixture is turned into ammonia. Thus , the gaseous coming out of the chamber contains NH3 and unreacted H2 and N2. These are then passed through condenser to condense only ammonia not H2 and N2. The liquefied ammonia is collected at the bottom from time to time. The other uncombined 
H2 and N2 is recycled and reprocedded. 






1 comment:

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